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The syn steroselectivity was based on the assumption that the oxidation step-the transformation of the carbon-boron bond to carbon-oxygen bond-took place with retention of configuration. More recent NMR studies of alkylboranes formed in hydroborating labeled alkenes indeed confirmed the validity of the earlier conclusion 51 Hydroboration of ex-pinene [Eq. (6.62)] is an excellent example demonstrating that the addition takes place on the less hindered side of the double bond. Similarly norbomene, when undergoing hydroboration with 9-BBN, gives 2-exa-norbomanol with 99.5% selectvity,344 whereas the gem-dimethyl group in 7,7-dimethylnorbornene brings about the reversal of the side of attack to yield the corresponding enda alcohol with 97% selectvity 52 Furthermore, even in the hydroboration of such sensitive compounds as ex-pinene and norbomene, no skeletal rearrangement has ever been observed during hydroboration. The characteristic features of hydroboration of alkenes-namely, regioselectivity, stereoselectivity, syn addition, and lack of rearrangement-led to the postulation of a concerted [2 + 2] cycloaddition of borane353 ,354 via four-center transition state 37. Kinetic studies, solvent effects, and molecular-orbital calculations are consistent with this model. As four-center transition states are unfavorable, however, the initial interaction of borane [or mentioned monobridged dimer, Eq. (6.56)] with the alkene probably involves an initial two-electron, three-center interaction 355 ,356(38, 39).

Un = 2 Un = 3 Un = 4 Un = 2 Un = 3 Un = 4 Un = 2 Un = 3 Un = 4 Un = 2 Un = 3 Un = 4 Un = 2 Un = 3 Un = 4

The Snapping Tolerance setting allows you to choose how close one object must be to another object before the first object automatically snaps to the second object. Set the Snapping Tolerance in points; the lower the number, the closer you must move the objects to each other. The Snapping Tolerance default is 4 points. That means when you re within 4 points to another object, your selected object snaps to the second object. I tend to stick with the default.

FIGURE 8.1 The Attributes panel allows you to set object attributes. Reverse Path Direction On Reverse Path Direction Off

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When you edit the SERIES formula and replace the range references with names, make sure that you replace only the range address and keep the sheet reference and the exclamation point that precedes the range reference. When you press Enter after making the modification, you ll find that Excel changes the reference in the SERIES formula to include the workbook name. If you don t want to edit the SERIES formula, you can use the Series tab of the Source Data dialog box to substitute the name for the range address.

The use of the Let( ) function to declare variables in calculation syntax has several potential advantages, especially in compound or complex expressions. Foremost among these advantages are n The capability to calculate a component value once and use it multiple places in the calc expression, thus reducing redundancy and minimizing the processor cycles required to evaluate the expression n The capability to break logic of a compound statement down into its elements and improve readability, simplicity, and clarity As an example of the elimination of redundancy, consider the following simple expression:

Remember, all examples from the book can be tried online by using the chapter and listing reference. For example, you can view the map created by Listing 7-1 by visiting http://maps .mcslp.com/examples/ch07-01.html.

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If you prefer not to clutter your screen with additional windows, Excel provides another option for viewing multiple parts of the same worksheet. Choosing View Window Split splits the active worksheet into two or four separate panes. The split occurs at the location of the cell pointer. If the cell pointer is in row 1 or column A, this command results in a 2-pane split. Otherwise, it gives you four panes. You can use the mouse to drag the individual panes to resize them. Figure 4.7 shows a worksheet split into two panes. Notice that row numbers aren t continuous. In other words, splitting panes enables you to display in a single window widely separated areas of a worksheet. To remove the split panes, choose View Window Split again.

Of interest, 1,5,9-cyclododecatriene prepared by trimerization of 1,3-butadiene undergoes only hydrogenation to cyclododecene. This reaction has potential since cyclododecene is a precursor to 1,12-dodecanedioic acid, a commercial polyamide intermediate. [RuCI 2(COh(PPh3h] gives 98-99% yield of cyclododecene under mild conditions (l25-160 C, 6-12 atm, in benzene with added PPh3 or in N,Ndimethylformamide ).143 [PtH(SnCI 3)(PPh3h] is one of the most selective catalysts to reduce conjugated and nonconjugated dienes and trienes to monoenes at elevated pressure. This behavior is best explained by supposing that the isomerization of nonconjugated bonds into conjugated position. The high selectivity for hydrogenation of dienes in the presence of monoenes arises from the exceptional stability of the TC-allyl complex of this catalyst.

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